HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-methyl-3-(methylamino)-4-nitrobenzamide → 4-Amino-N-methyl-3-methylamino-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-methyl-3-(methylamino)-4-nitrobenzamide | HCID 60144426 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 4-Amino-N-methyl-3-methylamino-benzamide | HCID 63356854 | 86% |
Reaction Steps
4-Amino-N-methyl-3-methylamino-benzamide (298 mg, 86%) was prepared by following General Procedure B starting from N-methyl-3-methylamino-4-nitro-benzamide (407 mg) and Pd/C (10% by weight, 40 mg). The crude product was used directly in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759535B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-b8c3d3a900554788a3e1c78cbe6c3a48 |
| Source note | uspto-grants-2014_06 |