HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoro-N-(2-methoxy-ethyl)-4-methylamino-5-nitro-benzamide → 5-Amino-2-fluoro-N-(2-methoxy-ethyl)-4-methylamino-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoro-N-(2-methoxy-ethyl)-4-methylamino-5-nitro-benzamide | HCID 67335417 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 5-Amino-2-fluoro-N-(2-methoxy-ethyl)-4-methylamino-benzamide | HCID 67333319 | — |
Reaction Steps
5-Amino-2-fluoro-N-(2-methoxy-ethyl)-4-methylamino-benzamide (72 mg) was prepared by following General Procedure B starting from 2-fluoro-N-(2-methoxy-ethyl)-4-methylamino-5-nitro-benzamide and Pd/C (10% by weight, 10 mg). Th crude product was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759535B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-cdb74bf054ce4606becf3b04888d648e |
| Source note | uspto-grants-2014_06 |