HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59395139, compound → HCID 67333436, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59395139 | HCID 59395139 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 67333436 | HCID 67333436 | 88.3% |
Reaction Steps
5-Amino-2-fluoro-4-methylamino-benzoic acid methyl ester (115 mg) was prepared by following General Procedure B starting from 2-fluoro-4-methylamino-5-nitro-benzoic acid methyl ester (150 mg) and Pd/C (10% by weight, 15 mg). The crude product was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759535B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-bb4a58489da942f2b8b4ab9e3527896c |
| Source note | uspto-grants-2014_06 |