HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → Methyl 2-methoxy-4-(methylamino)-5-nitrobenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 59395139 | HCID 59395139 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Methyl 2-methoxy-4-(methylamino)-5-nitrobenzoate | HCID 67331452 | 57% |
Reaction Steps
2-Methoxy-4-methylamino-5-nitro-benzoic acid methyl ester (120 mg) was prepared by following General Procedure A starting from 2-Fluoro-4-methylamino-5-nitro-benzoic acid methyl ester (200 mg) and sodium methoxide (190 mg) in DMF.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759535B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-3b6cff1b10a64bd39f4a83177e8c85db |
| Source note | uspto-grants-2014_06 |