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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 410792Generated: November 2, 2026

Diethylamine → 2-Diethylamino-4-methylamino-5-nitro-benzoic acid methyl ester

https://huagongshe.com/reaction/410792

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethylamineHCID 8021—
ReactantHCID 59395139HCID 59395139—
SolventDimethylformamideHCID 6228—
Product2-Diethylamino-4-methylamino-5-nitro-benzoic acid methyl esterHCID 67333294—

Reaction Steps

2-Diethylamino-4-methylamino-5-nitro-benzoic acid methyl ester (1.2 g) was prepared by following General Procedure A starting from 2-fluoro-4-methylamino-5-nitro-benzoic acid methyl ester (1.0 g) and diethylamine (683 uL) in DMF.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08759535B2
Source datasetuspto-grants-2014_06
ORD IDord-4ffcdd68e00b4846a811cb034a0d477b
Source noteuspto-grants-2014_06