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HRID410796

反应详情

EQUATION

反应方程式

HRID 410796 的结构方程式

REACTANTS

反应物

1
结构：CCOC(=O)c1cnc(NC)c([N+](=O)[O-])c1
HCID67333371

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1cnc(NC)c(N)c1
HCID67334125

未命名化合物

收率 91.6%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Pd]
催化剂HCID23938

Palladium

Pd

PROCEDURE

实验过程

5-Amino-6-methylamino-nicotinic acid ethyl ester (723 mg) was prepared by following General Procedure B starting from 6-methylamino-5-nitro-nicotinic acid ethyl ester (911 mg) and Pd/C (10% by weight, 90 mg). The crude product was used in the next step without further purification.

WORKUP

后处理

  1. customThe crude product was used in the next step without further purification