HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Methylamino)-3-nitrobenzonitrile → 3-Amino-4-(methylamino)benzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Methylamino)-3-nitrobenzonitrile | HCID 4600715 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 3-Amino-4-(methylamino)benzonitrile | HCID 2779731 | 0.1% |
Reaction Steps
3-Amino-4-methylamino-benzonitrile (1.23 mg) was prepared by following General Procedure B starting from 4-methylamino-3-nitro-benzonitrile (1.33 g) and Pd/C (10% by weight, 133 mg). The crude product was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759535B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-1f1675ebf3384b15baa6f0c22ffe8181 |
| Source note | uspto-grants-2014_06 |