HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → 64910-48-1
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Methyl 3-fluoro-4-nitrobenzonitrile | HCID 67335364 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 64910-48-1 | HCID 11019398 | — |
Reaction Steps
3-Methylamino-4-nitro-benzonitrile (1.58 mg) was prepared by following General Procedure A starting from methyl 3-fluoro-4-nitrobenzonitrile (1.66 g) and methylamine (2 M in THF, 10.0 mL) in DMF. The crude product was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759535B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-8abd64403b5e440bb66ed12735731c2f |
| Source note | uspto-grants-2014_06 |