HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-[4-(Methylamino)-3-nitrophenyl]ethan-1-one → 1-[3-Amino-4-(methylamino)phenyl]ethan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-[4-(Methylamino)-3-nitrophenyl]ethan-1-one | HCID 13175626 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 1-[3-Amino-4-(methylamino)phenyl]ethan-1-one | HCID 2779769 | 80.5% |
Reaction Steps
1-(3-Amino-4-methylamino-phenyl)-ethanone (66 mg) was prepared by following General Procedure B starting from 1-(4-methylamino-3-nitro-phenyl)-ethanone (97 mg) and Pd/C (10% by weight, 10 mg). The crude product was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759535B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-87f8acde2523403796d8989aa2db0b03 |
| Source note | uspto-grants-2014_06 |