HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Methanesulfonyl)-N-methyl-2-nitroaniline → 4-(Methanesulfonyl)-N~1~-methylbenzene-1,2-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Methanesulfonyl)-N-methyl-2-nitroaniline | HCID 121690 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 4-(Methanesulfonyl)-N~1~-methylbenzene-1,2-diamine | HCID 20551254 | 76% |
Reaction Steps
4-Methanesulfonyl-N1-methyl-benzene-1,2-diamine (76 mg) was prepared by following General Procedure B starting from (4-methanesulfonyl-2-nitro-phenyl)-methyl-amine (115 mg) and Pd/C (10% by weight, 10 mg). The crude product was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759535B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-672daa86a6b946c487977ede04cde21c |
| Source note | uspto-grants-2014_06 |