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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 410972Generated: November 1, 2026

HCID 86656889, compound → HCID 86656891, compound

https://huagongshe.com/reaction/410972

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86656889HCID 86656889—
SolventHydrochloric AcidHCID 313—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 86656891HCID 86656891258.5%

Reaction Steps

2-(6-Chloro-benzothiazol-2-ylamino)-1-(2-methylamino-ethyl)-1H-benzoimidazole-5-carboxylic acid [2-(2-hydroxy-ethoxy)-ethyl]-amide dihydrochloride (60 mg) was prepared by following General Procedure L starting from (2-{2-(6-chloro-benzothiazol-2-ylamino)-5-[2-(2-hydroxy-ethoxy)-ethylcarbamoyl]-benzoimidazol-1-yl}-ethyl)-methyl-carbamic acid tert-butyl ester (73 mg) in 4M HCl in dioxane (1 mL). LC/MS: m/z 488.5.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08759535B2
Source datasetuspto-grants-2014_06
ORD IDord-6384aecae1c1497299ca6f5621b2f1ea
Source noteuspto-grants-2014_06