HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67333336, compound → Ethyl 4-amino-3-(methylamino)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67333336 | HCID 67333336 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Ethyl 4-amino-3-(methylamino)benzoate | HCID 67332734 | 86.6% |
Reaction Steps
4-Amino-3-methylamino-benzoic acid ethyl ester (2.1 g) was prepared by following General Procedure B starting from 3-methylamino-4-nitro-benzoic acid ethyl ester (2.8 g) and Pd—C (560 mg) in methanol (25 mL).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759535B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-b5f84632771345e9a671e85022634d48 |
| Source note | uspto-grants-2014_06 |