HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 411046Generated: October 30, 2026
HCID 86656967, compound → HCID 86656968, compound
https://huagongshe.com/reaction/411046
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 86656967 | HCID 86656967 | — |
| Solvent | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Product | HCID 86656968 | HCID 86656968 | 91.4% |
Reaction Steps
2-(6-Chloro-benzothiazol-2-ylamino)-1-methyl-1H-benzoimidazole-5-carboxylic acid (2-oxo-ethyl)-amide (574 mg) was prepared starting from 2-(6-chloro-benzothiazol-2-ylamino)-1-methyl-1H-benzoimidazole-5-carboxylic acid (2,2-dimethoxy-ethyl)-amide (700 mg) in 4M HCl-dioxane (3 mL). The reaction was heated to 50° C. for 5 h. The solvent was evaporated to give crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08759535B2 |
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| Source dataset | uspto-grants-2014_06 |
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| ORD ID | ord-863b38c3e576448e976917517adddde6 |
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| Source note | uspto-grants-2014_06 |
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