関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 4-(Methylamino)-3-nitrobenzoic acid | HCID 283475 | — |
| 生成物 | 4-(Methylamino)-3-nitrobenzoyl chloride | HCID 17946449 | — |
反応手順
4-Methylamino-3-nitro-benzoyl chloride (4.3 g) was prepared starting from 4-methylamino-3-nitro-benzoic acid (4 g) in thionyl chloride (20 mL). The reaction was heated to 80° C. for 8 h. The solvent was evaporated to isolate pure compound without any further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08759535B2 |
|---|
| 出典データセット | uspto-grants-2014_06 |
|---|
| ORD ID | ord-cf67af8299fd443997516bc33d342552 |
|---|
| 出典メモ | uspto-grants-2014_06 |
|---|
