HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → 5-Chlorohexanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Hexanoic Acid | HCID 8892 | — |
| Reactant | N-Chloro-N,N-diisopropylamine | HCID 32745 | — |
| Product | 5-Chlorohexanoic acid | HCID 18541668 | — |
Reaction Steps
135 parts by mass of the caproic acid were added to 1,000 parts by mass of 84% sulfuric acid and an equivalent amount of N-chlorodiisopropylamine and were reacted for 5 hours at 25° C. to obtain 163 parts by mass of 5-chlorocaproic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06559275B2 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-e00c1458200e40adb14489b39ada7486 |
| Source note | uspto-grants-2003_05 |