HRID412011

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6422

未命名化合物

结构：CN(C)C(=O)COc1cc(Cl)ccc1C(=O)NCCN1CCN(C(=O)OC(C)(C)C)CC1

HCID11282784

未命名化合物

PRODUCTS

生成物

结构：CN(C)C(=O)COc1cc(Cl)ccc1C(=O)NCCN1CCNCC1.O=C(O)C(F)(F)F

HCID18536230

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

The product of step (c) (0.55 g) was dissolved in dichloromethane (15 ml) and trifluoroacetic acid (3 ml) added. After 1 hour the solvent was evaporated and the product obtained as a solid (0.9 g), m.p. 120-122° C.

WORKUP

后处理

customAfter 1 hour the solvent was evaporated