HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 18536231, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3,4-Dichlorobenzyl chloride | HCID 7609 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 18536253 | HCID 18536253 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18536231 | HCID 18536231 | — |
Reaction Steps
A solution of the product of step (a) (4.0 g), 3,4-dichlorobenzylchloride (1.9 ml) and triethylamine (9.0 ml) in N,N-dimethylformamide (20 ml) was stirred at room temperature. The solvent was removed and the residue purified by chromatography (dichloromethane:methanol, 1:0 to 4:1) to give an oil, which was treated with 1.0M ethereal hydrogen chloride to give the product as a solid (3.1 g), m.p. 240-41° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06562825B1 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-4fc7f075034c41b2b4a1f5482de75270 |
| Source note | uspto-grants-2003_05 |