HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 18536011, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 18536070 | HCID 18536070 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 18536011 | HCID 18536011 | — |
Reaction Steps
Through a solution of the product from Step D (7.71 g, 16.6 mmol) in 100 mL of ethyl acetate at 0° C. was bubbled anhydrous HCl gas for 10 minutes. After 30 minutes, the solution was concentrated in vacuo to provide the titled salt as a white foam which was used in the next reaction without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06562823B1 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-91f24bc3f2414c5e9632f67c619718f9 |
| Source note | uspto-grants-2003_05 |