反应详情

温度

350 °C

A zirconium phosphate film was prepared by adding a stoichometric amount of phosphate in the form of phosphoric acid to a solution of zirconium bound to PEI. The solution was then spin coated onto a glass slide and thermally treated at 1° C. to 120° C. with a dwell time of 30 minutes followed by heating to 350° C. at 1° C./minute with a dwell time of 30 minutes followed by heating to 450° C. at 1° C./minute with a dwell time of 1 hour and then cooling to 25° C.

1. additionthermally treated at 1° C. to 120° C. with a dwell time of 30 minutes
2. temperatureby heating to 450° C. at 1° C./minute with a dwell time of 1 hour
3. temperaturecooling to 25° C.