HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-tert-Butylcyclohexanone → HCID 53974670, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-tert-Butylcyclohexanone | HCID 7392 | — |
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 53974670 | HCID 53974670 | — |
Reaction Steps
This was prepared in the same manner as Lactone 1 except using 4-tert butylcyclohexanone (10 parts, 0.065 m ex. Aldrich), 3-chloroperoxybenzoic acid (17.5 parts, 0.0713M), sodium bicarbonate (11.5 parts, 0.143M) and dichloromethane (750 ml) in place of the 3-methyl cyclohexanone and amounts described for Lactone 1. The product was obtained as an oil (10.2 parts).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06562897B1 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-d5c2586ee21b41b29270bac94bacbffb |
| Source note | uspto-grants-2003_05 |