HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 85988586, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | Zirconium chloride (ZrCl4), (T-4)- | HCID 9856075 | — |
| Solvent | Nitromethane | HCID 6375 | — |
| Product | HCID 85988586 | HCID 85988586 | — |
Reaction Steps
1.2 g (5.1 mmol) of zirconium tetrachloride and 6.2 g (46.5 mmol) of aluminum trichloride were placed in a two-necked round-bottomed flask under an argon atmosphere. 410 ml of methylene chloride and 23 ml (25.9 g) of nitromethane were added (ratio Zr/nitro compound 1:82.5).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06562916B2 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-8b11187b3ec94ad888c5af91e5d386aa |
| Source note | uspto-grants-2003_05 |