HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 85988586, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | Zirconium chloride (ZrCl4), (T-4)- | HCID 9856075 | — |
| Solvent | Nitromethane | HCID 6375 | — |
| Product | HCID 85988586 | HCID 85988586 | — |
Reaction Steps
0.7 g (3.0 mmol) of zirconium tetrachloride and 7.6 g (57.0 mmol) of aluminum trichloride were placed in a two-necked round-bottomed flask under an argon atmosphere. 480 ml of methylene chloride and 3 ml (3.38 g) of nitromethane were added (ratio Zr/nitro compound 1:18.4).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06562916B2 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-ca34c9294c9d49d8a9d2939565ec2598 |
| Source note | uspto-grants-2003_05 |