HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 86585405, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Titanium Tetrachloride | HCID 24193 | — |
| Reactant | Zirconium chloride (ZrCl4), (T-4)- | HCID 9856075 | — |
| Solvent | Nitromethane | HCID 6375 | — |
| Product | HCID 86585405 | HCID 86585405 | — |
Reaction Steps
1.4 g (6.0 mmol) of zirconium tetrachloride and 10.207 g (53.8 mmol) of titanium tetrachloride were placed in a two-necked round-bottomed flask under an argon atmosphere. 480 ml of methylene chloride and 7 ml (7.89 g) of nitromethane were added (ratio Zr/nitro compound 1:21.5).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06562916B2 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-cb5f92a66fae4325a924ce2b1426830e |
| Source note | uspto-grants-2003_05 |