HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → Hafnium Tetrachloride nitromethane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Nitromethane | HCID 6375 | — |
| Reactant | Hafnium chloride (HfCl4) (6CI,8CI); Hafnium chloride; Hafnium tetrachloride; Hafnium(IV) chloride; Hafnium chloride (HfCl4), (T-4)- | HCID 9927068 | — |
| Product | Hafnium Tetrachloride nitromethane | HCID 22594783 | — |
Reaction Steps
17.9 g (55.9 mmol) of hafnium tetrachloride were placed in a two-necked round-bottomed flask under an argon atmosphere. 450 ml of methylene chloride and 32 ml (36.1 g) of nitromethane were added (ratio Hf/nitro compound 1:10.6).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06562916B2 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-d61610e868ec42f59c2298060b21dbb0 |
| Source note | uspto-grants-2003_05 |