反应详情

1-(Pyridin-4-yl)piperidine-4-carbamic acid benzyl ester (9.46 g) was hydrogenated using 7.5% palladium carbon (3.57 g) in ethanol (95 ml) solution at 3 atm over 3 hours. After completion of the reaction, the reaction mixture was filtered through celite, and the solvent was evaporated and the residue was dried under reduced pressure to give the title compound (5.38 g).

1. customover 3 hours
2. customAfter completion of the reaction
3. filtrationthe reaction mixture was filtered through celite
4. customthe solvent was evaporated
5. customthe residue was dried under reduced pressure