HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Thiophenethiol → HCID 18538833, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Thiophenethiol | HCID 522674 | — |
| Reactant | Tert-butyl 4-hydroxypiperidine-1-carboxylate | HCID 643502 | — |
| Product | HCID 18538833 | HCID 18538833 | — |
Reaction Steps
By a similar manner to Reference Example 35, 1-tert-butoxycarbonyl-4-hydroxypiperidine (1.01 g, 5.0 mmol) was reacted with 2-mercaptothiophene (0.70 g, 6.0 mmol) to give the titled compound as pale yellow oily substance (987 mg, 66%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06562978B1 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-62007ab2ab3b44748f00d416f41abf21 |
| Source note | uspto-grants-2003_05 |