Hydrochloric Acid → HCID 18538839, compound

Participants

Reaction Steps

The title compound of example 17 (1096 mg) dissolved in methanol was treated with 4N hydrogen chloride solution in ethyl acetate (0.75 mL) and the solvent was removed under reduced pressure. Diethyl ether was added to the residue, the resulting precipitate was collected by filtration, washed with diethyl ether, and dried under reduced pressure to afford the title compound (1060 mg) as a white amorphous solid.

Provenance & Evidence