HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 135856750, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | HCID 86597346 | HCID 86597346 | — |
| Reactant | 4-Propoxy-3-(5-methyl-4-oxo-7-propyl-3,4-dihydroimidazo[5,1-f][1,2,4]triazin-2-yl)-benzenesulphonyl chloride | HCID 135856736 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 135856750 | HCID 135856750 | — |
Reaction Steps
By the same method, starting with 42 mg (0.1 mmol) of 4-propoxy-3-(5-methyl-4-oxo-7-propyl-3,4-dihydro-imidazo[5,1-f][1,2,4]triazin-2-yl)-benzenesulphonyl chloride and 22 mg (0.6 mmol) of diethylamine, 42 mg (92%) of N,N-diethyl-3-(5-(methyl-4-oxo-7-propyl-3,4-dihydro-imidazo[5,1-f][1,2,4]triazin-2-yl)-4-propoxy-benzenesulphonamide are obtained. Rf=0.64 (dichloromethane/methanol=9:1)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06566360B1 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-6aeaf9bd407546edbed92e85626c5854 |
| Source note | uspto-grants-2003_05 |