HRID413094

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8021

Diethylamine

C4H11N

结构：CCCOc1ccc(S(N)(=O)=O)cc1-c1nn2c(CCC)ncc2c(=O)n1C

HCID86597346

未命名化合物

结构：CCCOc1ccc(S(=O)(=O)Cl)cc1-c1nn2c(CCC)nc(C)c2c(=O)[nH]1

HCID135856736

未命名化合物

PRODUCTS

生成物

结构：CCCOc1ccc(S(=O)(=O)N(CC)CC)cc1-c1nn2c(CCC)nc(C)c2c(=O)[nH]1

HCID135856750

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID21226129

未命名化合物

PROCEDURE

实验过程

By the same method, starting with 42 mg (0.1 mmol) of 4-propoxy-3-(5-methyl-4-oxo-7-propyl-3,4-dihydro-imidazo[5,1-f][1,2,4]triazin-2-yl)-benzenesulphonyl chloride and 22 mg (0.6 mmol) of diethylamine, 42 mg (92%) of N,N-diethyl-3-(5-(methyl-4-oxo-7-propyl-3,4-dihydro-imidazo[5,1-f][1,2,4]triazin-2-yl)-4-propoxy-benzenesulphonamide are obtained. Rf=0.64 (dichloromethane/methanol=9:1)

WORKUP

后处理

customare obtained