HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylphenyl boronic acid → HCID 22279314, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylphenyl boronic acid | HCID 2733267 | — |
| Reactant | HCID 22279276 | HCID 22279276 | — |
| Product | HCID 22279314 | HCID 22279314 | — |
Reaction Steps
This compound was made according to General Procedure XXIV in Example 406 from Compound 308 (Structure 16c of Scheme XXX, where R=H, R1=trilfuoromethyl) and commercially available 2-methylbenzeneboronic acid. Compound 742 was isolated as a white solid: 1H NMR (400 MHz, DMSO-d6) 12.42 (s, 1H), 7.68 (dd, J=9.6, 1.4, 1H), 7.53 (m, 2H), 7.33-7.23 (m, 4H), 7.04 (s, 1H), 2.51 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06566372B1 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-6070634a01cb4732b06c55196cdaf497 |
| Source note | uspto-grants-2003_05 |