HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 15739781, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Phenethyl bromide | HCID 7666 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Methoxybenzenethiol | HCID 12765 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 15739781 | HCID 15739781 | 95% |
Reaction Steps
A solution of 4-methoxy-benzene thiol (5.7 g), triethylamine (4.1 g) and 2-bromoethylbenzene (5.6 ml) in DMF (50 ml) at 0° C. was stirred for 2 h, then added to water and extracted with ether. The solvent was washed with water, 1M NaOH and brine, then dried and evaporated to give the title compound as colourless oil (8.9 g, 95%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06566384B1 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-f401f524186a42fd9d7ccd3b29d09277 |
| Source note | uspto-grants-2003_05 |