HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54008227, compound → HCID 9817918, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54008227 | HCID 54008227 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 9817918 | HCID 9817918 | 97.3% |
Reaction Steps
A mixture of 4.81 g 2-benzyloxycarbonylamino-3-(1,5,7-trimethyl-octyloxycarbonyloxy)-propionic acid benzyl ester, 250 ml methanol and a catalytic amount of 10% Pd/C was stirred six hours under an atmosphere of hydrogen. Filtration over Celite and evaporation under reduced pressure gave 2.69 g of colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06569411B2 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-74939db1f0bc486f945694f26ede0895 |
| Source note | uspto-grants-2003_05 |