HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethanolamine → L-Glutamic acid, N-(1-oxododecyl)-, compd. with 2,2',2''-nitrilotris[ethanol] (1:1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethanolamine | HCID 7618 | — |
| Reactant | N-Lauroyl-L-glutamic acid | HCID 93133 | — |
| Solvent | Water | HCID 962 | — |
| Product | L-Glutamic acid, N-(1-oxododecyl)-, compd. with 2,2',2''-nitrilotris[ethanol] (1:1) | HCID 104536 | — |
Reaction Steps
To the resulting liquid, triethanolamine was added so as to convert 50% of the carboxyl group of N-lauroyl-L-glutamic acid to its salt, and further pure water was added thereto so as to make a solid content 30% by weight. The liquid was mixed under stirring to obtain an aqueous solution of triethanolamine N-lauroyl-L-glutamate. A yield (as acid) of N-lauroyl-L-glutamic acid, a tertiary butanol concentration and a free fatty acid content were found to be 90.5%, 60 ppm by weight and 8.3% by weight, respectively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06569829B1 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-82630c8d52284c73ae0202fc59d4bbea |
| Source note | uspto-grants-2003_05 |