Glutaric anhydride → HCID 4150750, compound

Participants

Reaction Steps

There are added to 10 cm3 of dioxane, 1.517 g of glutaric anhydride and then, dropwise, 1.75 cm3 of N-(2-aminoethyl)morpholine. Stirring is continued at 20° C. for 0.75 hours. The white solid formed is filtered, washed successively with dioxane and diethyl ether, and then dried at 20° C. (90 Pa) to give 1.94 g of 5-(2-morpholinoethylamino)-5-oxopentanoic acid in the form of a white solid melting at 96° C.

Provenance & Evidence