HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 22611021, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | Sodium sulfide nonahydrate | HCID 73972 | — |
| Reactant | HCID 18522031 | HCID 18522031 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 22611021 | HCID 22611021 | — |
Reaction Steps
A mixture of 2-nitro-N-(4-(2-thiazolylamino)phenyl)aniline (1.2 g, 3.8 mmol), sodium sulfide nona hydrate (4.61, 19.2 mmol), ammonium chloride (1.03 g, 19.2 mmol) and ethanol (40 ml) was stirred at reflux for 40 h. Water (50 ml) was added, the mixture was stirred and filtered. Yield 0.49 g, 46%. M.p. 184-186° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06569880B2 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-031abc84e8544dfa85846c5813f7f54a |
| Source note | uspto-grants-2003_05 |