HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 491837, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 9798485 | HCID 9798485 | — |
| Catalyst | Nickel Dichloride | HCID 24385 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 491837 | HCID 491837 | — |
Reaction Steps
The compound of Example 22 (0.86 mmol, 0.3 g) was dissolved in methanol and treated with NiCl2 and NaBH4 (17.2 mmol) using the procedure set forth in Example 40. The named product was purified over silica (m.p. 142° C.-143° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06569890B2 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-06ba413ad5114898acc3404ccc4e0482 |
| Source note | uspto-grants-2003_05 |