HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanoacetamide → HCID 21282644, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanoacetamide | HCID 7898 | — |
| Reactant | HCID 21282659 | HCID 21282659 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21282644 | HCID 21282644 | — |
Reaction Steps
In a manner analogous to that described in Example 2, by reacting 2,3-dichlorobenzyl azide with cyanoacetamide there is obtained 5-amino-1-(2,3-dichlorobenzyl)-1H-1,2,3-triazole-4-carboxamide having a melting point of 224°-226° (from ethanol). The starting material can be produced from 2,3-dichlorobenzyl alcohol as starting material by halogenation, for example with phosphorus tribromide, and reaction with sodium azide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04789680 |
| Source dataset | uspto-grants-1988_12 |
| ORD ID | ord-f78d030ed44f4c9d84dad5b4c4c1b530 |
| Source note | uspto-grants-1988_12 |