HRID414146
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
CONDITIONS
反应条件
- 温度
- 140 °C
PROCEDURE
实验过程
In a similar manner to that described in Example 1, o-allylphenol (134 g), 1,3-bisglycidylresorcinol (115.1 g), triphenylethylphosphonium iodide (0.75 g) and methylglycolate (145 g) were reacted at 100° C. for 13 hours. The solvent and excess o-allylphenol were removed by heating at 140° C. finally in vacuo. The yield of adduct was 227.9 g and it showed a viscosity of 280 mPa.s at 70° C.
WORKUP
后处理
- customwere reacted at 100° C. for 13 hours
- customThe solvent and excess o-allylphenol were removed
- customat 70° C.