HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → (1H-indene-3-yl)methylamine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-(aminomethyl)-2,3-dihydro-1H-inden-1-ol | HCID 14348695 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | (1H-indene-3-yl)methylamine hydrochloride | HCID 14348696 | 85% |
Reaction Steps
Two and three-tenth g of 1-hydroxyindanylmethylamine is dissolved in 100 ml of ethanol saturated with HCl . Reaction mixture is refluxed overnight. It is cooled to room temperature and volatiles are evaporated under reduced pressure. The residue is stirred with 300 ml anhydrous ether. Precipitated solid is filtered and dried affording 2.2 g (85%) of the (1H-indene-3-yl)methylamine hydrochloride having a melting point of 245° C. decomp.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04791103 |
| Source dataset | uspto-grants-1988_12 |
| ORD ID | ord-d92c469402694c57b0e870cd7160263c |
| Source note | uspto-grants-1988_12 |