Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | Methyl 2-pentenoate | HCID 5364718 | — |
| Product | HCID 21282412 | HCID 21282412 | — |
Reaction Steps
A mixture of 171 g of methyl 2-trans-pentenoate and 106.5 g of pyrrolidine was heated for 20 hours at 100° C. After distillation over a Vigreux column, 198.7 g (72% of theory) of methyl 3-pyrrolidinovalerate of boiling point 65° C./0.4 mbar, nD20 =1.4580, were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04791220 |
|---|
| Source dataset | uspto-grants-1988_12 |
|---|
| ORD ID | ord-8c83315f67fe41fc94a1e1befc7c9c9c |
|---|
| Source note | uspto-grants-1988_12 |
|---|
