1,2-Dibromoethane → HCID 15606616, compound

Participants

Reaction Steps

30 g of 4-methoxythiophenol, 20.2 g of ethylene bromide, 40 g of potassium carbonate, and 40 ml of dimethylformamide were placed in a 300 ml flask, and stirred for 3 hours as the interior of the flask was maintained at a temperature of from 50° C. to 60° C. The reaction mixture was poured into ice-cold water to deposit crystals. The crystals were recrystallized from methanol/ethyl acetate 1/1 (volume ratio) mixture. Melting point: 108°-110° C.

Provenance & Evidence