HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → N-[2-(9-anthryloxy)ethyl]phthalimide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-(9-Anthryloxy)ethyl chloride | HCID 21280820 | — |
| Reactant | Phthalimide potassium salt | HCID 24194345 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | N-[2-(9-anthryloxy)ethyl]phthalimide | HCID 14373233 | — |
Reaction Steps
2-(9-Anthryloxy)ethyl chloride (7.0 g) and potassium phthalimide (2.8 g) were heated to 130° C. in dimethylformamide (70 ml) for 7 hours. The cooled solution was added to water and extracted with ethyl acetate. The extract was dried and evaporated to yield N-[2-(9-anthryloxy)ethyl]phthalimide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04792551 |
| Source dataset | uspto-grants-1988_12 |
| ORD ID | ord-99badd7e088745e7b0623acc33b34423 |
| Source note | uspto-grants-1988_12 |