HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphoric Acid → HCID 86122419, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphoric Acid | HCID 1004 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 416338 | HCID 416338 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86122419 | HCID 86122419 | — |
Reaction Steps
A twofold stoichiometric excess of 3% phosphoric acid in methanol is added to a methanolic solution of 1.0 g. of 1-(9-anthryloxy)-3-dimethylaminopropane. Diethyl ether is added until precipitation is complete. The product is filtered, washed with ether, air dried and recrystallized to give 1-(9-anthryloxy)-3-dimethylaminopropane phosphate, m.p. 196°-200° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04792551 |
| Source dataset | uspto-grants-1988_12 |
| ORD ID | ord-bdbe9fde43d8473fbf3b322b15f61767 |
| Source note | uspto-grants-1988_12 |