HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 414493Generated: October 25, 2026
Benzyl Bromide → N,O-Dibenzylhydroxylamine
https://huagongshe.com/reaction/414493
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | O-Benzylhydroxylamine | HCID 102313 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N,O-Dibenzylhydroxylamine | HCID 11063773 | 33.7% |
Reaction Steps
A mixture of 4 g of O-benzylhydroxylamine, 4.28 g of benzyl bromide, and 12 g of K2CO3 in 50 ml of ethanol was stirred at 50° C. overnight. After removal of organic solvent, water was added to the residue and the mixture was then extracted with ethyl acetate. The combined extracts were dried and evaporated to give 4 g of crude product. Purification by dry column chromatography gave 1.8 g of oily product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04792560 |
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| Source dataset | uspto-grants-1988_12 |
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| ORD ID | ord-addcd505782e4867bc2047d110324372 |
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| Source note | uspto-grants-1988_12 |
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