HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetaldehyde → HCID 53844222, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetaldehyde | HCID 998 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Benzyloxyamine hydrochloride | HCID 102312 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53844222 | HCID 53844222 | 85.3% |
Reaction Steps
A mixture of 5 g of phenylacetaldehyde, 6.7 g of O-benzylhydroxylamine hydrochloride, and 3 g of potassium carbonate in 30 ml of aqueous methanol (1:1) was refluxed for 2 hours. The aqueous solution was extracted with ethyl acetate and the organic solution was dried and evaporated to give 8 g of crude product which was used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04792560 |
| Source dataset | uspto-grants-1988_12 |
| ORD ID | ord-009a3675a0c945c2ad86344464a09c1b |
| Source note | uspto-grants-1988_12 |