HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 21281403, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 21281389 | HCID 21281389 | — |
| Reactant | Phthalimide potassium salt | HCID 24194345 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21281403 | HCID 21281403 | — |
Reaction Steps
A solution of 1-(4-biphenyloxy)-6-chlorohexane (10.0 g) and potassium phthalimide (9.0 g) in dimethylformamide (100 ml) was heated at 140° C. for 4 hours. The cooled solution was poured into water (900 ml) and filtered to yield N-[6-(4-biphenyloxy) hexyl]phthalimide. (b) In a similar manner, but using the appropriate corresponding optionally substituted 1-(3- or 4-biphenyloxy)-ω-chloroalkane, obtained as described in Preparation 4, the following compounds of Formula C were prepared:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04792570 |
| Source dataset | uspto-grants-1988_12 |
| ORD ID | ord-bfcb2722765b4cfb876af515ac29a558 |
| Source note | uspto-grants-1988_12 |