HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 13957280, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-[([1,1'-Biphenyl]-4-yl)oxy]butan-1-amine--hydrogen chloride (1/1) | HCID 13957281 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 13957280 | HCID 13957280 | — |
Reaction Steps
1.0 g of 4-(4-biphenyloxy)-1-aminobutane hydrochloride suspended in 50 ml of ether is stirred with a twofold stoichiometric excess of dilute aqueous potassium carbonate solution until the salt is completely dissolved. The organic layer is then separated, washed twice with water, dried over magnesium sulfate and evaporated to yield 4-(4-biphenyloxy)-1-aminobutane as the free base.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04792570 |
| Source dataset | uspto-grants-1988_12 |
| ORD ID | ord-935f77006a134f998740a44b49023a2e |
| Source note | uspto-grants-1988_12 |