HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 21281345, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 70418201 | HCID 70418201 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21281345 | HCID 21281345 | — |
Reaction Steps
7-(4-biphenyloxy)-1-dimethylaminoheptane acetate (1.0 g) is dissolved in 50 ml water containing a stoichiometric equivalent of sulfuric acid, and the solution evaporated to dryness. The product is suspended in ethanol and filtered, air dried and recrystallized from methanol/acetone to yield 7-(4-biphenyloxy)-1-dimethylaminoheptane bisulfate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04792570 |
| Source dataset | uspto-grants-1988_12 |
| ORD ID | ord-9c9140c1ec3f4179b0c7f2a550a92398 |
| Source note | uspto-grants-1988_12 |