HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 21280350, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 3350368 | HCID 3350368 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 21280350 | HCID 21280350 | — |
Reaction Steps
A solution of 15.6 g (0.06 mole) of 3-methylthio-1-trifluoroacetylimidazo[1,5-a]pyridine (J. Bourdais et al. J. Het. Chem. 17, 1351, 1980) in 750 ml of chloroform is cooled to 5° C. 30.6 g (0.132 mole) of m-chloroperbenzoic acid is added in the course of approximately 1 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04794120 |
| Source dataset | uspto-grants-1988_12 |
| ORD ID | ord-2397f6b49f84450aaa112edef08639f2 |
| Source note | uspto-grants-1988_12 |