m-Chloroperbenzoic acid → HCID 21280350, compound

HRID 414713Notes

Reaction equation

HRID 414713 reaction equation
[CH3:1][S:2][C:3]1[N:7]2[CH:8]=[CH:9][CH:10]=[CH:11][C:6]2=[C:5]([C:12](=[O:17])[C:13]([F:16])([F:15])[F:14])[N:4]=1.ClC1C=CC=C(C(OO)=[O:26])C=1>C(Cl)(Cl)Cl>[CH3:1][S:2]([C:3]1[N:7]2[CH:8]=[CH:9][CH:10]=[CH:11][C:6]2=[C:5]([C:12](=[O:17])[C:13]([F:16])([F:14])[F:15])[N:4]=1)=[O:26]

Participants

4

Reactant 2

HCID 70297m-Chloroperbenzoic acidHCID 3350368HCID 3350368, compound

Product 1

HCID 21280350HCID 21280350, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

A solution of 15.6 g (0.06 mole) of 3-methylthio-1-trifluoroacetylimidazo[1,5-a]pyridine (J. Bourdais et al. J. Het. Chem. 17, 1351, 1980) in 750 ml of chloroform is cooled to 5° C. 30.6 g (0.132 mole) of m-chloroperbenzoic acid is added in the course of approximately 1 h.

Sources & evidence

ORD record
ord-2397f6b49f84450aaa112edef08639f2
Source dataset
uspto-grants-1988_12
Patent number
US04794120

Reaction notes

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